Physico-chemical Analysis of Industrial Catalysts: A Practical Guide to CharacterisationJohn Lynch Editions TECHNIP, 2003 - 305 pages This book describes the principal physico-chemical techniques for characterising the catalysts used in searching for new active phases, optimising the formulation and monitoring industrial production. Based on courses given at the Institut Francias du Peole for research technicians in the fields of kinetics and catalysis, this book covers useful basic theory and provides numerous examples of industrial applications. This guide is an essential companion for technicians and chemical engineers whose work requires an understanding of the fields of application, including the capabilities and the limits of today's complex characterisation techniques.Contents: Introduction. 1. d104ural characterisation of catalysts. 2. Atomic absorption spectrometry. 3. Atomic emission spectroscopy. 4. X-ray fluorescence. 5. X-ray photoelectron spectroscopy. 6. Ion impact analysis. 7. Scanning electron microscopy. 8. Elemental analysis in the electron microprobe. 9. Transmission electron microscopy. 10. X-ray diffraction and small-angle scattering. 11. Exafs. 12. Infrared absorption spectrometry. 13. Nuclear magnetic resonance. 14. Thermal analysis methods. Index |
Table des matières
Introduction | 1 |
Arc Emission Spectrography | 48 |
Inductively Coupled Plasma ICP Emission Spectrometry | 68 |
XRAY PHOTOELECTRON SPECTROSCOPY | 87 |
SCANNING ELECTRON MICROSCOPY | 119 |
ELEMENTAL ANALYSIS IN THE ELECTRON MICROPROBE | 143 |
XRAY DIFFRACTION AND SMALLANGLE SCATTERING | 193 |
29 | 208 |
INFRARED ABSORPTION SPECTROMETRY | 237 |
37 | 265 |
NUCLEAR MAGNETIC RESONANCE | 273 |
40 | 276 |
THERMAL ANALYSIS METHODS | 291 |
| 303 | |
Autres éditions - Tout afficher
Physico-chemical Analysis of Industrial Catalysts: A Practical Guide to ... John Lynch Affichage d'extraits - 2003 |
Expressions et termes fréquents
absorbed absorption acid adsorbed alumina aluminium angle approximately atomic number backscattered backscattered electron beam binding energy calibration carbon catalyst characteristic chemical shift cm-¹ composition compounds concentration level contrast corresponding crystal curve depends detection limits detector determine diagram diameter diffraction dispersive distribution emission emitted energy levels EXAFS example excitation faujasite Figure frequency hydrotalcite hydrotreatment infrared intensity ionisation ions light elements matrix effects measurement metal method micrometres microscope molecules monochromator nanometres obtained optical oxide particles peak phase photoelectron photon planes plasma pore possible powder probe pyridine qualitative quantitative analysis radiation ratio resolution sample scanning scanning electron microscope scattering secondary electron images secondary electrons sensitivity shows signal solid solution specific spectra spectrometer spectroscopy spectrum standard structure STUDY OF CATALYSTS surface technique temperature tion transmission electron microscopy vacuum variation vibration voltage wave-number wavelength X-ray fluorescence zeolite